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How to make ethyl acetate | Part 1 (Synthesis + Raman analysis)

10,978 views October 25, 2018 10:46

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ChannelChemistry 4all

Description from the creator

Today, we will be making some ethyl acetate by means of a classic esterification reaction.The final product turned out to be contaminated with significant amounts of ethanol, and so we will try to purify the product obtained in a future video.

Additional notes:

-The raman spectra were taken with a professional 785 nm raman equipment, since the power supply of my DIY raman spectrometer is not working right now.

-Software employed for the analysis of the raman spectra: Spectragryph (effemm2.de/spectragryph/).

This is my first video narrated with my "real" voice, let me know in the comments section whether you prefer this voice or the "synthetic" one.

About this tutorial

Chemistry 4all published this 10:46 video tutorial on October 25, 2018. It has been watched 10,978 times on YouTube.

Duration
10:46
Published
October 25, 2018
Views
10,978
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Further reading

  • Ethyl acetate - Wikipedia en.wikipedia.org

    Production and synthesis. Ethyl acetate was first synthesised by Count de Lauraguais in 1759 by distilling a mixture of ethanol and acetic acid.. In 2004, an estimated 1.3 million tonnes were produced worldwide.

  • Synthesis of Ethyl Acetate | Hobby Chemistry hobbychemistry.wordpress.com

    Introduction Ethyl Acetate is a broadly used solvent. It has a sweet smell similar to pear drops (according to Wikipedia). I'm going to be making it using the classical Fischer Esterification reaction.

  • Ethyl Acetate Production and Manufacturing Process | ICIS icis.com

    The main method to manufacture ethyl acetate involves the esterification of ethanol with acetic acid although some is produced by the catalytic condensation of acetaldehyde with alkoxides.

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